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Contributors | ||
Preface | ||
1 | Transuranium Elements: Their Impact on Science and Technology | 2 |
Historical Viewpoints | ||
2 | Transuranium Elements: A Half Century | 10 |
3 | Discovery of Neptunium | 50 |
4 | Chemistry of Plutonium Revealed | 56 |
5 | The Transuranium Elements: Members of the 5f Series | 63 |
6 | Early Days in the "Met Lab": Organization and Planning in Scientific Research | 78 |
7 | Early Chemical Contributions in Los Alamos | 86 |
8 | "Dry Chemistry" and Initiatory Thermodynamics at the Metallurgical Laboratory | 93 |
Nuclear Physics and Chemistry | ||
9 | Nuclear and Chemical Properties of Elements 103, 104, and 105 | 104 |
10 | Production of Plutonium-237 | 116 |
11 | Mass and Alpha Spectrometry for the Determination of the Half-Life of [superscript 241]Pu | 121 |
12 | Plutonium Determination by Isotope Dilution Technique with Mass and Alpha Spectrometry | 126 |
13 | Highly Enriched Isotope Samples of Uranium and Transuranium Elements for Scientific Investigation | 131 |
Spectroscopy, Photophysics, and Photochemistry | ||
14 | Unusual High-Temperature Behavior of Neptunium and Plutonium Systems | 138 |
15 | Magnetic and Optical Properties of Np and Pu Ions and Compounds | 145 |
16 | Detection and Speciation of Trace Amounts of Neptunium and Plutonium | 159 |
17 | Photochemical Removal of NpF[subscript 6] and PuF[subscript 6] from UF[subscript 6] Gas Streams | 168 |
18 | Vibronic Interaction and Crystal Structure Distortion in Cm[superscript 4+] in CeF[subscript 4] | 181 |
19 | Ion-Ion Interaction and Energy Transfer of 4+ Transuranium Ions in Cerium Tetrafluoride | 187 |
20 | Investigation of Neptunium(V) Reduction to Neptunium(IV) by Semiconductor Photocatalysis | 195 |
Chemistry | ||
21 | f-Element Compound Synthesis Employing Powerful Halogenating Agents | 202 |
22 | Cationic Speciation in Nonaqueous Media: Uranium, Neptunium, and Plutonium in Oxidation States III and IV | 213 |
23 | The Chemistry of Uranium(VI), Neptunium(VI), and Plutonium(VI) in Aqueous Carbonate Solutions | 225 |
24 | The Lanthanides and Actinides: Among Other Groups of Elements in Mendeleev's System | 233 |
25 | Transuranium Organometallic Elements: The Next Generation | 239 |
26 | Gas-Phase Uranium Ion Reactions with 2,4,6-Tri-t-butylphenol and 1,3,5-Tri-t-butylbenzene: Fourier Transform-Ion Cyclotron Resonance Mass Spectrometry | 247 |
27 | Characterization of the Plutonium-Water Reaction: Reaction Kinetics Between 200 and 350 [degree] C | 251 |
Separations and Thermodynamics | ||
28 | Reduction of Neptunium(VI) by Organic Compounds | 262 |
29 | The Complexation Behavior of Neptunium and Plutonium with Nitrilotriacetic Acid | 276 |
30 | Catalyzed Electrolytic Plutonium Oxide Dissolution: The Past 17 Years and Future Potential | 288 |
31 | Aqueous Chemistry of Neptunium and Plutonium: Studies in the USSR | 305 |
32 | Recovery of Neptunium, Plutonium, and Americium from Highly Active Waste: Trialkylphosphine Oxide Extraction | 318 |
33 | 3-Phenyl-4-benzoyl-5-isoxazolone: A Novel Extractant for Pu(IV) and Am(III) | 331 |
Materials Physics | ||
34 | Metallic Covalency in Actinide Compounds | 338 |
35 | Nuclear Hyperfine Techniques in the Study of Transuranium Materials | 345 |
36 | Surface Electronic Structure and Chemisorption of Plutonium and Uranium | 365 |
37 | Magnetization Measurements on Single Crystals of Neptunium Monopnictides | 378 |
Materials Chemistry | ||
38 | High-Pressure Phases and Compressibility of Neptunium and Plutonium Compounds | 396 |
39 | Electronic, Structural, and Transport Properties of (Almost) Rare-Earth-Like Actinide Hydrides | 404 |
40 | Hydrolysis of Plutonium: Plutonium-Oxygen Phase Diagram | 416 |
41 | The Pivotal Position of Plutonium in the Systematics of Actinide Metals and Compounds | 426 |
42 | Defect Chemistry of Plutonium Oxides | 440 |
43 | Formation of Lithium Plutonates by the Reaction of Lithium Nitrate and Lithium Hydroxide with PuO[subscript 2] | 451 |
44 | Mechanisms of the Rapid Dissolution of Plutonium Dioxide in Acidic Media under Oxidizing or Reducing Conditions | 457 |
45 | Complex Formation of the Lanthanides and Actinides in Lower Oxidation States | 469 |
46 | Synthesis and Identification of [actual symbol not reproducible] and Preparation of PuCl[subscript 3] | 481 |
47 | Homogeneous Oxalate Precipitation of Pu(III) | 489 |
Analytical Chemistry | ||
48 | Transuranium Reference Measurements and Reference Materials | 496 |
49 | Airborne Transuranium Elements: Progress in Rapid Detection | 507 |
50 | Development of Neptunium and Plutonium Chemistry: Contribution of Electrochemical Research | 515 |
51 | A New Chemical Assay Standard for Plutonium | 524 |
Appendix: Papers Presented But Not Included in Book | 533 | |
Index | 536 |
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