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Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach Book

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach
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  • Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach
  • Written by author Jeffrey H. Simpson
  • Published by Elsevier Science, August 2008
  • Ideal for advanced undergraduate and graduate courses in organic spectroscopy, this book provides the analytical skills and methodologies needed to assign nuclear magnetic resonances to known and unknown molecular structures. Part I covers the essential k
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Ch. 1 Introduction 1

Ch. 2 Instrumental Considerations 19

Ch. 3 Data Collection, Processing, and Plotting 51

Ch. 4 [superscript 1]H and [superscript 13]C Chemical Shifts 83

Ch. 5 Symmetry and Topicity 95

Ch. 6 Through-Bond Effects: Spin-Spin (J) Coupling 101

Ch. 7 Through-Space Effects: The Nuclear Overhauser Effect (NOE) 137

Ch. 8 Molecular Dynamics 151

Ch. 9 Strategies for Assigning Resonance to Atoms Within a Molecule 157

Ch. 10 Strategies for Elucidating Unknown Molecular Structures 183

Ch. 11 Simple Assignment Problems 199

Ch. 12 Complex Assignment Problems 233

Ch. 13 Simple Unknown Problems 271

Ch. 14 Complex Unknown Problems 299

Glossary of Terms 333

Index 349


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