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Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17- Book

Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-
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Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-, Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical , Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989
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  • Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989
  • Written by author Robert E. Botto, Yuzo Sanada
  • Published by American Chemical Society, 1999/02/25
  • Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical
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Preface
Overviews
1 Quantitation in [superscript 13]C NMR Spectroscopy of Carbonaceous Solids 3
2 [Superscript 1]H NMR Spectroscopy: Approaches for Carbonaceous Solids 27
3 Solid Materials Research with NMR and Dynamic Nuclear Polarization Spectroscopy 45
4 Advances in Electron Nuclear Double Resonance Spectroscopy 65
5 Strategies for Measurement of Electron Spin Relaxation 91
6 Multifrequency Electron Paramagnetic Resonance Spectroscopy 107
7 High-Temperature Electron Spin Resonance and NMR Methods Applied to Coal 139
NMR Spectroscopy
8 Diffusion-Coupled Relaxation and the Submicroscopic Structure of Bituminous Coals 175
9 [Superscript 13]C NMR Spectroscopy of Pyridine and Alkylpyridines Sorbed onto Coal 201
10 Distortion-Free [superscript 13]C NMR Spectroscopy in Coal: [superscript 1]H Rotating-Frame Dynamic Nuclear Polarization and [superscript 1]H-[superscript 13]C Cross-Polarization 217
11 Proton Magnetic Resonance Thermal Analysis of Argonne Premium Coals 229
12 Multivariate Statistical Analysis and Pattern Recognition: Principal-Component Analysis of Coal Solid-State NMR Relaxation Times 253
13 Structural Parameters of Argonne Coal Samples: Solid-State [superscript 13]C NMR Spectroscopy 269
14 Characterization of Coal Liquefaction Residues by Solid-State [superscript 13]C NMR Spectroscopy 281
15 [Superscript 1]H NMR Spectroscopy and Spin-Lattice Relaxation of Argonne Premium Coals 295
16 High-Field NMR Studies of Argonne Premium Coals 311
17 Solid-State [superscript 13]C NMR Studies on Coal and Coal Oxidation 323
18 Measurement of Spin Lattice Relaxation in Argonne Premium Coal Samples 341
19 Quantitation of Protons in the Argonne Premium Coals by Solid-State [superscript 1]H NMR Spectroscopy 359
20 Bloch-Decay and Cross-Polarization - Magic-Angle Spinning [superscript 13]C NMR Study of the Argonne Premium Coals: Effects of High-Speed Spinning 377
21 High-Resolution [superscript 1]H NMR Studies of Argonne Premium Coals 401
22 Measurement of [superscript 13]C Chemical-Shift Anisotropy in Coal 419
Electron Paramagnetic Resonance Spectroscopy
23 2-mm Band and X-Band Electron Spin Resonance and Electron Spin-Echo Investigations of Some Carbonaceous Materials 443
24 Electron Spin Resonance, Electron Nuclear Double Resonance, and Electron Spin-Echo Spectroscopic Studies of Argonne Premium Coals 451
25 Electron Paramagnetic Resonance Spin-Probe Studies of Porosity in Solvent-Swelled Coal 467
26 Dynamic In Situ 9-GHz Electron Paramagnetic Resonance Studies of Argonne Premium Coal Samples 483
27 Electron Magnetic Resonance of Standard Coal Samples at Multiple Microwave Frequencies 507
28 Novel Characterization of Argonne Premium Coals with Electron Donors or Acceptors by Electron Paramagnetic Resonance Spectroscopy 529
29 Electron Paramagnetic Resonance and Electron Spin-Echo Spectroscopy of Argonne Premium Coals 539
30 Pulsed Electron Nuclear Double Resonance Spectroscopy of Argonne Premium Coals 561
31 Temperature Dependence of the Electron Paramagnetic Resonance Intensity of Whole Coals: The Search for Triplet States 581
32 Measurement of Electron Dipolar Fields and Dynamics in Solids 605
33 Advanced Magnetic Resonance Techniques Applied to Argonne Premium Coals 629
Author Index 647
Affiliation Index 647
Subject Index 648


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Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-, 
Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical , Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989

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Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-, 
Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical , Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989

Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-

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Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-, 
Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical , Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-22, 1989

Magnetic Resonance of Carbonaceous Solids: Developed by a Symposium Sponsored by the 1989 International Chemical Congress of Pacific Basin Societies, Honolulu, Hawaii, December 17-

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